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标题：Critical applications of SW 846 US EPA methods to evaluation of marine samples quality
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作者：Silvério, Patrícia Ferreira ; Gonçalves, Cristina ; Taniguchi, Satie 等
期刊名称：Brazilian Journal of Oceanography
印刷版ISSN：1679-8759
电子版ISSN：1982-436X
出版年度：2010
卷号：58
期号：spe3
页码：49-56
DOI：10.1590/S1679-87592010000700007
出版社：Instituto Oceanográfico da Universidade de São Paulo
摘要：Technical evaluation of analytical data is of extreme relevance considering it can be used for comparisons with environmental quality standards and decision-making as related to the management of disposal of dredged sediments and the evaluation of salt and brackish water quality in accordance with CONAMA 357/05 Resolution.It is, therefore, essential that the project manager discusses the environmental agency's technical requirements with the laboratory contracted for the follow-up of the analysis underway and even with a view to possible re-analysis when anomalous data are identified.The main technical requirements are: (1) method quantitation limits (QLs) should fall below environmental standards; (2) analyses should be carried out in laboratories whose analytical scope is accredited by the National Institute of Metrology (INMETRO) or qualified or accepted by a licensing agency; (3) chain of custody should be provided in order to ensure sample traceability; (4) control charts should be provided to prove method performance; (5) certified reference material analysis or, if that is not available, matrix spike analysis, should be undertaken and (6) chromatograms should be included in the analytical report.Within this context and with a view to helping environmental managers in analytical report evaluation, this work has as objectives the discussion of the limitations of the application of SW 846 US EPA methods to marine samples, the consequences of having data based on method detection limits (MDL) and not sample quantitation limits (SQL), and present possible modifications of the principal method applied by laboratories in order to comply with environmental quality standards.
关键词：Sedimento;Métodos SW 846;Limite de quantificação;Água salgada e salobra;Interferências
其他关键词：sediment;SW 846 methods;Quantitation limit;Salt and brackish water;interferences