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  • 标题:Quantitative Analysis of Semicrystalline Blends SAXS Data: Theoretical Modeling versus Linear Correlation Function
  • 本地全文:下载
  • 作者:Mohamed Fatnassi ; Fadhel Ben Cheikh Larbi ; Jean Louis Halary
  • 期刊名称:International Journal of Polymer Science
  • 印刷版ISSN:1687-9422
  • 电子版ISSN:1687-9430
  • 出版年度:2010
  • 卷号:2010
  • DOI:10.1155/2010/829752
  • 出版社:Hindawi Publishing Corporation
  • 摘要:This paper compares the results yielded by two methods of small-angle X-ray scattering data analysis for semicrystalline polymer blends. The first method is based on the use of a theoretical modeling for isotropic samples and a subsequent curve fitting. The second one is a more familiar method, based on the calculation of the linear one-dimensional correlation function. The experimental material considered for this purpose deals with a series of semi-crystalline blends of poly(vinylidene fluoride) and poly(methyl methacrylate), with a PVDF content covering the range 50 wt%–100 wt%. The results obtained by both calculation methods are systematically confronted to the crystallinity degrees deduced from wide angle X-ray scattering patterns.
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