文章基本信息

标题：Efficient filtration system for paraffin-catalyst slurry separation
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作者：Mohammad Khodagholi ; Mohammad Hemmati ; Ali Pour 等
期刊名称：Chemical Industry and Chemical Engineering Quarterly
印刷版ISSN：1451-9372
出版年度：2013
卷号：19
期号：2
页码：295-301
DOI：10.2298/CICEQ120226063K
出版社：Association of the Chemical Engineers
摘要：The filtration efficiency for separating liquid paraffin (or water) from a slurry consisting of 25 weight% spherical alumina in a Slurry Bubble Column Reactor (SBCR) comprised of a cylindrical tube of 10 cm diameter and 150 cm length was studied. Various differential pressures (ΔP) were applied to two separate tubular sintered metal stainless steel filter elements with nominal pore size of 4 and 16μm. The experimental results disclosed that the rate of filtrations increased on applying higher differential pressure to the filter element. Albeit this phenomenon is limited to moderate ΔPs and for ΔP more than 1 bar is neither harmful nor helpful. The highest filtration rates at ΔPs higher than 1 bar were 170 and 248 ml/minute for 4 and 16μm respectively. Using water as the liquid in slurry the rate of filtration enhanced to 4 folds, and this issue reveals impact of viscosity on filtration efficiency clearly. In all situations, the total amount of particles present in the filtrate part never exceeded a few parts per million (ppm). The statistical analysis of the SEM image of the filtrate indicated that by applying higher pressure difference to the filter element the frequency percent of larger particle size increases. The operation of filter cake removing was performed with back flashing of 300 ml of clean liquid with pressures of 3-5 bar of N2 gas.
关键词：Fischer-Tropsch Synthesis; Wax-Catalyst Slurry Separation; Slurry Bubble Column Reactor; cake filtration; solid-liquid separation; sintered metal