文章基本信息

标题：Simpler and Faster Spectrophotometric Determination of Diclofenac Sodium in Tablets,Serum and Urine Samples
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作者：Abdul Rauf Khaskheli ; Sirajuddin ; Kamran Abro 等
期刊名称：Pakistan Journal of Analytical & Environmental Chemistry
印刷版ISSN：1996-918X
电子版ISSN：2221-5255
出版年度：2009
卷号：10
期号：1
页码：53-59
语种：English
出版社：National Centre of Excellence in Analytical Chemsitry
摘要：This work describes a simple,sensitive,rapid and economical analytical procedure for direct spectrophotometric evaluation of diclofenac sodium (DS) using aqueous medium without using a chemical reagent. Parameters like time,temperature,acidic and basic conditions and interference by analgesic drugs were studied for a 5µg ml-1 solution of DS at 276 nm. Under optimized parameters,a linear working range of 0.1–30 g ml-1 with regression coefficient of 0.9998 and lower detection limit of 0.01 g ml-1 was obtained. The method was applied for DS contents in tablets,serum and urine samples..
关键词：Diclofenac sodium;UV-Visible spectrophotometer;tablets;serum;urine