文章基本信息

标题：Elaboration and Viscosimetric, Viscoelastic and Rheological Studies of a New Hexafunctional Polyepoxide Polymer : Hexaglycidyl Ethylene of Methylene Dianiline
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作者：Hsissou R. ; El Bouchti M. ; El Harfi A. 等
期刊名称：Journal of Materials and Environmental Science
印刷版ISSN：2028-2508
出版年度：2017
卷号：8
期号：12
页码：4349-4361
DOI：10.26872/jmes.2017.8.12.480
出版社：University of Mohammed Premier Oujda
摘要：In this work, we studied the viscosimetric, viscoelastic and rheological behavior of a new hexafunctional epoxy polymer: hexaglycidyl ethylene of methylene dianiline (HGEMDA) which is synthesized in the laboratory and its natural phosphate-based composite as loading. In the first stage, after the synthesis of the macromolecular matrix (HGEMDA), we crosslinked and formulated it in order to produce a thermosetting technological composite material in the presence of natural phosphate loadings at different percentages (0% , 5%, 10% and 15%) by adding methylene dianiline (MDA) as hardener. Secondly, we studied the viscosimetric properties of this epoxy prepolymer by the use of an Ubbelohd VB-1423 capillary viscosimeter and the viscoelastic and rheological properties by the use of a RHM01 type rheometer -RD HAAKE. It was very important to specify the influence of natural phosphate in the rheological behavior of nanocomposites based on macromolecular matrix and natural phosphate.
关键词：Nanocomposite; viscosimetric; viscoelastic; rheological behavior; methylene dianiline; natural phosphate