文章基本信息

标题：The dry ashing - AAS method and the microwave digestion -ICP-MS method for determination of lead in plastic packaging bag
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作者：Haipeng Mi ; Xilin Zhou ; Bo Liang 等
期刊名称：IOP Conference Series: Earth and Environmental Science
印刷版ISSN：1755-1307
电子版ISSN：1755-1315
出版年度：2019
卷号：300
期号：5
页码：1-7
DOI：10.1088/1755-1315/300/5/052024
出版社：IOP Publishing
摘要：A pink plastic packaging bag sample from a enterprise was preliminarily screened via X-ray fluorescence spectroscopy method (XRF), it was found that the lead content exceeded the limit of relevant national standards. Subsequently, the total lead content in the packaging bag was determined via atomic absorption spectrophotometry pretreated by dry ashing method (DA-AAS) and inductively coupled plasma–mass spectrometry with microwave digestion method (MD-ICP-MS), respectively. The working curve equations were obtained by linear least squares method with the calculated linear correlation coefficients r above 0.9998 and the relative standard deviation (RSD) of the determination results from 1.0% to 6.2%, which was in good agreement with the result of XRF.