文章基本信息

标题：Study on novel structure of 4-amino-2-chloropyridine bis(salicylato)borate hydrate
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作者：Yongmei Yan ; Haixing Liu ; Lintong Wang 等
期刊名称：IOP Conference Series: Earth and Environmental Science
印刷版ISSN：1755-1307
电子版ISSN：1755-1315
出版年度：2019
卷号：300
期号：5
页码：1-6
DOI：10.1088/1755-1315/300/5/052004
出版社：IOP Publishing
摘要：A novel complex C14H8BO6. (C5H6ClN2). (H2O) has been synthesized from a hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. Orthorhombic, Pccn. a=16.6736(13) Å, b=29.447(3) Å, c=8.1366(6) Å, α=β=γ=90°. V=3995.0(6) Å3. Z=8. R1 = 0.0567, wR2 = 0.1624, T=293(2)K. The B atom is coordinated by four O atoms from two salicylic acid molecular. The molecular structure stabilized by the O-H...O and O-H...N hydrogen-bonding interactions.