文章基本信息

标题：Synthesis and Structural Characterization of 2-(2-Aminophenyl) Benz imidazole
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作者：Meili Zhao ; Dandan Lin ; Qian Liang 等
期刊名称：IOP Conference Series: Earth and Environmental Science
印刷版ISSN：1755-1307
电子版ISSN：1755-1315
出版年度：2019
卷号：252
期号：2
页码：1-5
DOI：10.1088/1755-1315/252/2/022034
出版社：IOP Publishing
摘要：A Benz imidazole derivative, 2-(2-aminophenyl) Benz imidazole, was synthesized by simple one-pot synthesis method. Its structure was characterized by X-ray single-crystal structural analysis. The results of crystal analysis are C₁₃H₁₁N₃, M _r = 209.25, orthorhombic, space group Pbca, a = 7.7679 (16) Å, b = 11.855(2) Å, c = 22.552(5) Å, α = β = γ = 90°, V = 2076.7(7) Å³, Z = 8, Dc = 1.339 g cm⁻³, μ = 0.083 mm⁻¹, F (000) = 880, and final R ₁ = 0.0365, ωR ₂ = 0.0947. The 2-(2-aminophenyl) Benz imidazole molecule is co-planar. The title compound molecules form 1D chained structure and 2D layered structure by the interaction of intermolecular N-H.N hydrogen bonds.