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  • 标题:Fragment-Based Discovery of Pyrimido[1,2-b]indazole PDE10A Inhibitors
  • 本地全文:下载
  • 作者:Ayaka Chino ; Ryushi Seo ; Yasushi Amano
  • 期刊名称:Chemical and Pharmaceutical Bulletin
  • 印刷版ISSN:0009-2363
  • 电子版ISSN:1347-5223
  • 出版年度:2018
  • 卷号:66
  • 期号:3
  • 页码:286-294
  • DOI:10.1248/cpb.c17-00836
  • 语种:English
  • 出版社:The Pharmaceutical Society of Japan
  • 摘要:

    In this study, we report the identification of potent pyrimidoindazoles as phosphodiesterase10A (PDE10A) inhibitors by using the method of fragment-based drug discovery (FBDD). The pyrazolopyridine derivative 2 was found to be a fragment hit compound which could occupy a part of the binding site of PDE10A enzyme by using the method of the X-ray co-crystal structure analysis. On the basis of the crystal structure of compound 2 and PDE10A protein, a number of compounds were synthesized and evaluated, by means of structure–activity relationship (SAR) studies, which culminated in the discovery of a novel pyrimidoindazole derivative 13 having good physicochemical properties.

  • 关键词:phosphodiesterase10A inhibitor;fragment-based drug discovery;schizophrenia;combinatorial synthesis;pyrimido[1,2-b]indazole
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