文章基本信息

标题：X線回折データからの多変量解析法による塩酸メタンフェタミンと塩酸エフェドリン混合比の決定
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作者：奥山修司 ; 三井利幸 ; 藤村義和等
期刊名称：Journal of Health Science
印刷版ISSN：1344-9702
电子版ISSN：1347-5207
出版年度：1992
卷号：38
期号：2
页码：176-180
DOI：10.1248/jhs1956.38.176
出版社：The Pharmaceutical Society of Japan
摘要：Ten samples of powder mixtures containing known quantities of methamphetamine·HCL and ephedrine·HCl were measured by X-ray diffraction. The respective I/I_O values of 19 peales were selected for calibration. The data was used for the multivariate analyses including a cluster analysis, and a cluster analysis derived from the deviation and a principal component analysis. Subsequently the approximate values of the methamphetamine·HCl contents of unknown samples were determined from the 12×19 matrix. The accurate methamphetamine·HCl contents of unknown samples were calculated from the principal component score. Differences between the theoretical and calculated values of 10 samples ranged from -1.4 to 1.7% (the respective methamphetamine·HCl contents are 3.9, 14.5, 20.2, 34.4, 44.0, 49.8, 60.0, 75.2, 96.1 and 99.1%).
关键词：methamphetamine·HCl content;ephedrine·HCl;multivariate analysis;X-ray diffraction