文章基本信息

标题：ガスクロマトグラフィーによる血液中のディプテレックス(0,0-ジメチル-2,2,2-トリクロロ-1-ヒドロキシエチルホスホネイト)の定量
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作者：神津公 ; 駒沢重光 ; 高沼重義等
期刊名称：Journal of Health Science
印刷版ISSN：1344-9702
电子版ISSN：1347-5207
出版年度：1976
卷号：22
期号：2
页码：91-93
DOI：10.1248/jhs1956.22.91
出版社：The Pharmaceutical Society of Japan
摘要：Dipterex in blood was determined by gas-liquid chromatography with a flame photometric detector on 2.0-m glass column packed with 25% carbowax 20 M at 180°. Determination was carried out successfuly by using trimethyl phosphate as an internal standard. Dipterex was extracted from blood with ether after salting-out with magnesium sulfate and adjusting to pH 5.8. The clean-up procedure suitable for the extract was carried out by a column packed with silica gel containing 15% water by weight. The component was eluted with acetone : methanol (90 : 10) mixture. The recovery of Dipterex added to blood was 94.3%.