文章基本信息

标题：大気中クロルエチレンのガスクロマトグラフィーにおける妨害物質の分離
本地全文：下载
作者：青山大器
期刊名称：Journal of Health Science
印刷版ISSN：1344-9702
电子版ISSN：1347-5207
出版年度：1977
卷号：23
期号：2
页码：95-99
DOI：10.1248/jhs1956.23.95
出版社：The Pharmaceutical Society of Japan
摘要：A simple method is described for separation of interference by co-existing methyl chloride and acetaldehyde in gas chromatographic quantitation of low levels of chloroethylene in air. Methyl chloride and acetaldehyde were successfully separated from chloroethylene by FID-gas chromatography using a column of 5.5% Ucon oil LB 550 X and Porapak QS. Relative deviation of peak area was found less than 5% on reproducibility of quantitative analysis, and the limit of detection was 1-4 ppb of chloroethylene.
关键词：chloroethylene;methyl chloride;acetaldehyde;separation of interference;quantitation of low levels of chloroethylene in air;gas chromatography;precolumn;Porapak QS;Ucon oil LB 550 X