文章基本信息

标题：ガスクロマトグラフィーによる血中マラチオンの定量
本地全文：下载
作者：神津公 ; 赤沼一弘 ; 松沢恒友等
期刊名称：Journal of Health Science
印刷版ISSN：1344-9702
电子版ISSN：1347-5207
出版年度：1983
卷号：29
期号：6
页码：423-426
DOI：10.1248/jhs1956.29.6_423
出版社：The Pharmaceutical Society of Japan
摘要：Malathion in the blood was determined by gas liquid chromatography with a flame thermionic detector on 1.0 m glass column packed with 10% DC-200 at 225°C. The blood was haemolyzed by the addition of 9 parts of water, subjected to modified Extrelut[○!R] column and malathion was eluted from the column with n-hexane. Determination was carried out successfully by the internal standard method using cyanophenphos. The calibration curve of malathion in ethyl acetate solution (0.5-4.0 μg/ml) showed a straight line. The recovery of malathion added to the blood (4.0 μg/ml) was 100.32±2.07%. Malathion in the blood of a suicide was identified by gas liquid chromatography-chemical ionization mass spectrometry and the content was 1.03 μg/ml.
关键词：blood malathion;gas chromatography;modified Extrelut[○!R] column;cyanophenphos;mass fragmentgraphy