文章基本信息

标题：ヒト血液中からの農薬カルタップの抽出
本地全文：下载
作者：三井利幸 ; 藤村義和
期刊名称：Journal of Health Science
印刷版ISSN：1344-9702
电子版ISSN：1347-5207
出版年度：1986
卷号：32
期号：4
页码：305-307
DOI：10.1248/jhs1956.32.305
出版社：The Pharmaceutical Society of Japan
摘要：The selection of best solvent for extracting cartap from human blood was examined. The experimental procedures were as follows ; One ml of blood sample was added to 0.5 ml of 8% sodium hydroxide solution in a 15 ml test tube. The sample was extracted with 5 ml of cyclohexane by shaking for 3 min, and centrifuged at 3000 rpm for 2 min. The cartap extracted with cyclohexane was derivatized by reacting with 3, 4-dimethyl benzyl chloride. The 3, 4-dimethyl benzyl derivative of cartap was spectrophotometrically measured by using tropaeoline OO as an ion-associating reagent. For the extraction of cartap from blood sample no interference could be observed with the compounds, such as Fe (III), Cu (II), glycine, L-phenylalanine, urea, glucose, lactose.
关键词：agricultural chemical cartap;human blood;spectrophotometric determination