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  • 标题:Synthesis and characterization of 1- and 2-monoglycerides of anteiso fatty acids
  • 本地全文:下载
  • 作者:B. Serdarevich ; K. K. Carroll
  • 期刊名称:JLR Papers In Press
  • 印刷版ISSN:0022-2275
  • 电子版ISSN:1539-7262
  • 出版年度:1966
  • 卷号:7
  • 期号:2
  • 页码:277-284
  • 语种:English
  • 出版社:American Society for Biochemistry and Molecular Biology
  • 摘要:The branched-chain fatty acids d -(+)-12-methyltetradecanoic acid (C15 anteiso) and d -(+)-14-methylhexadecanoic acid (C17, anteiso) were isolated from the lipids of Listeria monocytogenes and their 1- and 2-monoglycerides were prepared. Reaction intermediates and products were purified without isomerization by column chromatography. Thin-layer chromatography on Florisil impregnated with boric acid and nuclear magnetic resonance were used in characterizing the 1- and 2-monoglycerides. The value of the latter method for analyzing glyceride structure is discussed.
  • 关键词:bacterial lipids ; anteiso fatty acids ; 1- and 2-monoglycerides ; synthesis ; chromatography ; column ; thin-layer ; silica gel-boric acid ; gas-liquid ; nuclear magnetic resonance ; isomerization ; glyceride structure ; monocytosis
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