文章基本信息

标题：24,25-epoxysterols. Differentiation of 24R and 24S epimers by 13C nuclear magnetic resonance spectroscopy.
本地全文：下载
作者：G T Emmons ; W K Wilson ; G J Schroepfer 等
期刊名称：JLR Papers In Press
印刷版ISSN：0022-2275
电子版ISSN：1539-7262
出版年度：1989
卷号：30
期号：1
页码：133-138
语种：English
出版社：American Society for Biochemistry and Molecular Biology
摘要：The 24R and 24S epimers of the acetates of 24,25-epoxycholesterol and 24,25-epoxylanosterol have been prepared and purified by preparative normal phase high performance liquid chromatography. Neither pair of epimers could be differentiated by 1H NMR. However, the 13C NMR spectra of the epimeric pairs were sufficiently different to permit samples of individual epimers to be assigned as 24R or 24S.