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  • 标题:Synthesis of 24-heteroatom-substituted cholestanols.
  • 本地全文:下载
  • 作者:M D Rahman ; H M Seidel ; R A Pascal
  • 期刊名称:JLR Papers In Press
  • 印刷版ISSN:0022-2275
  • 电子版ISSN:1539-7262
  • 出版年度:1988
  • 卷号:29
  • 期号:11
  • 页码:1543-1548
  • 语种:English
  • 出版社:American Society for Biochemistry and Molecular Biology
  • 摘要:Short syntheses of 24-thia-5 alpha,20 xi-cholestan-3 beta-ol, 24-methyl-24-aza-5 alpha,20 xi-cholestan-3 beta-ol, and 24-nor-5 alpha,20 xi-cholan-3 beta-ol from 3 beta-hydroxy-5 alpha-pregnan-20-one are described. The products and synthetic intermediates have been fully characterized by the results of proton NMR, infrared, and high and low resolution mass spectral studies.
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