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  • 标题:Bile acids. OV. 2,2-Dimethoxypropane: an esterifying agent preferred to diazomethane for chenodeoxycholic acid.
  • 本地全文:下载
  • 作者:R Shaw ; W H Elliott
  • 期刊名称:JLR Papers In Press
  • 印刷版ISSN:0022-2275
  • 电子版ISSN:1539-7262
  • 出版年度:1978
  • 卷号:19
  • 期号:6
  • 页码:783-787
  • 语种:English
  • 出版社:American Society for Biochemistry and Molecular Biology
  • 摘要:Artifacts formed by methylation of chenodeoxycholic acid with diazomethane are identical to the synthetic 3alpha- and 7 alpha-monomethyl ethers of methyl chenodeoxycholate. The extent of formation of these artifacts with time has been studied. No detectable artifacts were found with 2,2-dimethoxypropane as the methylating agent.
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