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  • 标题:Artifacts produced during acid-catalyzed methanolysis of sterol esters.
  • 本地全文:下载
  • 作者:J K Kramer ; H W Hulan
  • 期刊名称:JLR Papers In Press
  • 印刷版ISSN:0022-2275
  • 电子版ISSN:1539-7262
  • 出版年度:1976
  • 卷号:17
  • 期号:6
  • 页码:674-676
  • 语种:English
  • 出版社:American Society for Biochemistry and Molecular Biology
  • 摘要:Sterol esters were transesterified within 1 hr using either acid or base catalysts. Acid-catalyzed methanolysis of sterol esters with HCl, H2SO4, or BF3 leads to the formation of two artifacts derived from the sterol portion of the molecule; they were identified as dehydrated and methoxylated derivatives of sterols. These two artifacts were not produced using a base-catalyzed methanolysis with NaOCH3.
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