文章基本信息

标题：Potential of liquid chromatography–atmospheric pressure chemical ionisation tandem mass spectrometry for determination of fosetyl-aluminium residues in dried hops
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作者：Poustka J. ; Hajšlová J. ; Holadová K. 等
期刊名称：Czech Journal of Food Sciences
印刷版ISSN：1212-1800
电子版ISSN：1805-9317
出版年度：2004
卷号：22
期号：1
页码：24-28
DOI：10.17221/3403-CJFS
出版社：Czech Academy of Agricultural Sciences
摘要：New analytical procedure for the determination of fosetyl-aluminium in hop cones (also called “hops”) was developed. Liquid chromatography–atmospheric pressure chemical ionisation tandem mass spectrometry (LC–APCI-MS/MS) allowed a highly selective determination of this fungicide which facilitated the sample preparation. The sufficiently low detection limit (1 mg/kg of dried hops) with the acceptable method performance characteristics (RSD 9%, recovery 76% – at the level of 10 mg/kg) complies with the need to inspect the observance of maximal residual limit 100 mg/kg. The application of LC-MS technique thus provided an effective way of fosetyl-aluminium determination in the complex hops matrix.
关键词：fosetyl-aluminium; pesticide residues; hops analysis; liquid chromatography; mass spectrometry