文章基本信息

标题：Determination of vinyl chloride monomer in food contact materials by solid phase microextraction coupled with gas chromatography/mass spectrometry
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作者：Jordáková I. ; Dobiáš J. ; Voldich M. 等
期刊名称：Czech Journal of Food Sciences
印刷版ISSN：1212-1800
电子版ISSN：1805-9317
出版年度：2003
卷号：21
期号：1
页码：13-17
DOI：10.17221/3472-CJFS
出版社：Czech Academy of Agricultural Sciences
摘要：The present study concerns the optimisation of the headspace solid phase microextraction (HS/SPME) combined with gas chromatography/mass spectrometry (GC/MS) for the vinyl chloride monomer determination. Samples of PVC materials were analysed using the Carboxen/Polydimethylsiloxane (CX/PDMS) 75 µm fibre. For this fibre, the achieved limit of detection was 0.05 µg/kg, and that of quantification 0.17 µg/kg, respectively, with RSD 5%. The levels of VCM found ranged from 0.29 to 0.44 mg/kg, in the case of foil, the VCM content determined was 3.65 mg/kg which means that the maximal limit allowed was exceeded.
关键词：migration; solid phase microextraction (SPME); vinyl chloride monomer