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  • 标题:New macrocyclic compounds using organotin complexes as intermediates: synthesis and characterization
  • 本地全文:下载
  • 作者:Harminder Kaur ; Kanav Dhir ; Bharti Mittu
  • 期刊名称:International Journal of Fundamental and Applied Sciences
  • 印刷版ISSN:2278-1404
  • 出版年度:2012
  • 卷号:1
  • 期号:2
  • 页码:30-33
  • 出版社:BioMedAsia
  • 摘要:Background and Aim: A new series of macrocyclic compounds 1-4 have been synthesized using tin as templates. Method:Tin templates are formed by refluxing the solution of dibutyltin (IV) oxide with orthophenylenediamine (L1H), 4-chlorocatechol (L2H), butane dithiol (L3H) and 3-carboxypropyldisulphide (L4H). Results:The reaction is visualized by cleavage X-Sn-X (X= oxygen/ nitrogen/ sulphur atom) bond of tin template when treated with adipoyldichloride. Conclusion:The compounds 1-4 are characterized with the aid of elemental analyses, IR and NMR (1H, 13C) studies which confirmed their proposed framework.
  • 关键词:dibutyltin (IV) oxide; orthophenylenediammine (L1H); 4-chlorocatechol (L2H); butane dithiol ; (L3H); 3-carboxypropyldisulphide (L4H).
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