摘要:The monodisperse Fe-Co-Ni trimetalic powder has been synthesized by polyol method. The synthesized nanoparticles were characterized by scanning electron microscopy (SEM), energy dispersive Xray spectroscopy (EDS) and Fourier transform infrared spectroscopy (FT-IR).The morphological features as studied using SEM revealed that the nanoparticles were agglomerated, crispy with porous. Keywords: Nanoparticles; Polyol method; Characterization; SEM; FTIR.