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  • 标题:発色現像主薬の薄層クロマトグラフィーによる定性分析
  • 本地全文:下载
  • 作者:束原 宏和
  • 期刊名称:日本写真学会誌
  • 印刷版ISSN:0369-5662
  • 电子版ISSN:1884-5932
  • 出版年度:1969
  • 卷号:32
  • 期号:1
  • 页码:7-12
  • DOI:10.11454/photogrst1964.32.7
  • 出版社:The Society of Photographic Science and Technolgy of Japan
  • 摘要:

    It was found that Thin-Layer Chromatography is useful as one of the methods to indentify the chemical structure of dye-foming developing agents. The best results were obtained on silica gel layers among various adsorbents. Diethylparamine, Droxychrome, CD-III and Agfa's dye-forming developing agent, the most popular ones, were most successfully separated when they were developed on a silica gel (WAKOGEL B-5) layer with diethylether. The method of detection described in the present work is that the developed layer is sprayed with the aqueous solution of phenol and immediately with the ammoniacal solution of silver nitrate in the light room. Dye-forming developing agents are detected as bluish colored spots, while black-and-white deveroping agents appear as dark spots. This experimental technique can be directly applied both to aqueous solutions of mineral acid salts of dye-formig developing agents and to color developers which are usually alkaline aqueous solutions.

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