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  • 标题:ピレスロイド系農薬の薄層クロマトグラフィー,ガスクロマトグラフィー質量分析法および液体クロマトグラフィー質量分析法による一斉分析
  • 本地全文:下载
  • 作者:地中 啓 ; 岩室 嘉晃 ; 飯尾 麗子
  • 期刊名称:日本法科学技術学会誌
  • 印刷版ISSN:1880-1323
  • 电子版ISSN:1881-4689
  • 出版年度:2008
  • 卷号:13
  • 期号:2
  • 页码:177-186
  • DOI:10.3408/jafst.13.177
  • 出版社:Japanese Association of Forensic Science and Technology
  • 摘要:

      Simultaneous analytical methods for 33 pyrethroids by thin layer chromatography (TLC), gas chromatography/mass spectrometry (GC/MS) and liquid chromatography/mass spectrometry (LC/MS) have been developed. The detection limits of the pyrethroids were 1 μg or less by TLC, 10-100 pg by GC/MS (SIM mode) and 5-200 pg by LC/MS (SIM mode, except for transfluthrin (2 ng)). The proposed methods were applicable to the analysis of the pyrethroids mixed into drinks and foods.

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