Mass measurement using a relay feedback system was studied experimentally. The measurement system has an on-off relay with hysteresis and switches force acting on the object in relation to its velocity. Such nonlinear control induces a limit cycle in the feedback system. The mass of the object is determined from the period of this limit cycle. The apparatus manufactured for experimental study uses two voice coil motors (VCM's), one of which is for driving the object and the other is for generating prescribed disturbances. The effects of system parameters and disturbances on measurement accuracy were examined experimentally.