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  • 标题:Disinfection By-Products of para-Hydroxybenzoate Esters (Parabens): Synthesis and Mass Spectrometric Study
  • 本地全文:下载
  • 作者:Masanori Terasaki ; Masakazu Makino
  • 期刊名称:Journal of Health Science
  • 印刷版ISSN:1344-9702
  • 电子版ISSN:1347-5207
  • 出版年度:2009
  • 卷号:55
  • 期号:4
  • 页码:631-635
  • DOI:10.1248/jhs.55.631
  • 出版社:The Pharmaceutical Society of Japan
  • 摘要:A simple and efficient procedure for the chlorination of para -hydroxybenzoate esters (parabens) with sulfuryl chloride is described. Fourteen monochlorinated or dichlorinated parabens were synthesized and their mass spectrometric characteristics were determined. This work enabled the definitive identification and quantification of the chlorinated parabens in environmental samples.
  • 关键词:disinfection by-product;paraben;chlorination;standard material;gas chromatography-mass spectrometry
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