摘要:In this paper, the composite ZnS/MoS2 was obtained via two steps including solvothermal methods. The as-synthesized sample was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and UV-Vis. diffuse reflectance spectra (DRS). The photocatalytic activity of the product was evaluated through photocatalytic degradation of Rhodamine B (Rh B) under UV-Vis. light irradiation; the electrical conductivity of ZnS/MoS2 composites was significantly improved compared to ZnS, MoS2, respectively. The results showed that the ZnS/MoS2 composite photocatalyst possesses better photocatalytic activity in degrading Rh B than the single ZnS or the single MoS2. The better photocatalytic properties may be due to the synergetic effect of two semiconductors, because of which electrons and holes were separated effectively. And its specific microstructure played an active role in evaluating photocatalytic performance.